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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3040102 Date: 04/09/2003 Page: 24 <br /> Project Name: OLVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 1 ST QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-9 Lab Samp ID: 33857-011 <br /> Descr/Location: MW-9 Recd Date: 04/01/2003 <br /> Sample Date: 03/28/2003 Prep Date: 04/07/2003 <br /> Sample Time: 1018 Analysis Date: 04/07/2003 <br /> Matrix: Water QC Batch: WM8110015 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 1. PQL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> tent-Butyl alcohol (TBA) 4.6 10. PQL ND UG/L 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 0.5 5, PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 107.0% 1 <br /> Toluene-d8 77-150 SMEA 112.0% 1 <br /> Dibromofluoromethane 57-156 SMEA 110.0% 1 <br /> Approvea by: 41 r3 uate: <br />