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f) <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3040102 Date: 04/09/2003 Page: 13 <br /> Project Name: OLVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 1 ST QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: EW-1 Lab Samp ID: 33857-012 <br /> Descr/Location: EW-1 Recd Date: 04/01/2003 <br /> Sample Date: 03/28/2003 Prep Date: 04/07/2003 <br /> Sample Time: 1404 Analysis Date: 04/07/2003 <br /> Matrix: Water QC Batch: WMS110015 <br /> Basis: Not Filtered Notes: BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 15. 50. PQL 62a UG/L 50 <br /> Ethyl tert-butyl ether(ETRE) 25. 250. PQL ND UG/L 50 <br /> tert-Amyl methyl ether(TAME) 15. 250. PQL ND UG/L 50 <br /> DI-isopropyl ether(DIPE) 25. 250. PQL ND UG/L 50 <br /> tert-Butyl alcohol (TBA) 230. 500. PQL ND UG/L 50 <br /> 1,2-Dichloroethane 15. 250. PQL 41 a UG/L 50 <br /> 1,2-Dibromoethane 25. 250. PQL 31 Q UGIL 50 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 94.6% 1 <br /> Toluene-d8 77-150 SMSA 89.5% 1 <br /> Dibromofluoromethane 57-156 SMEA 93.1% 1 <br /> BH: Reporting limits raised due to high level of non-target analytes <br /> Approvea by: '� - __ uate: 4 f {O/D3 <br />