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' O <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2123101 Date: 0 1 11 0120 03 Page: 2 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-1R Lab Samp ID: 32743-007 <br /> Descr/Location: MW-1R Recd Date: 12/31/2002 <br /> Sample Date: 12/30/2002 Prep Date: 01/02/2003 <br /> Sample Time: 1400 Analysis Date: 01/02/2003 <br /> Matrix: Water QC Batch: WMS21862 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 1. PQL 12 UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 4.6 10. PQL 12 UG/L 1 <br /> 1,2-Dichloroethane 0.3 5. PQL 22 UG/L 1 <br /> 1,2-Dibromoethane 1 0.5 5. PQL 11. UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 99.9% 1 <br /> Toluene-d8 77-150 SMEA 103.2% 1 <br /> Dibromofluoromethane 57-156 SMEA 109.2° 1 <br /> Approved by: Date: JC <br />