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a <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> ab Report No.: H2123101 Date: 01/10/2003 Page: 1 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-1 Lab Samp ID: 32743-006 <br /> DescNLocation: Mw-1 Recd Date: 12/31/2002 <br /> Sample Date: 12/30/2002 Prep Date: 01/03/2003 <br /> Sample Time: 1338 Analysis Date: 01/03/2003 <br /> Matrix: Water QC Batch: WMS21863 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 3. 10. PQL 74Q UGIL 10 <br /> Ethyl tert-butyl ether(ETBE) 5. 50. PQL ND UGIL 10 <br /> tert-Amyl methyl ether(TAME) 3. 50. PQL ND UGIL 10 <br /> Di-isopropyl ether(DIPE) 5. 50. PQL ND UGIL 10 <br /> tert-Butyl alcohol (TBA) 46. 100. PQL 32Q UGIL 10 <br /> 1,2-Dichloroethane 3. 50. PQL 26a UGIL 10 <br /> 1,2-Dibromoethane 5. 50. POLL 16a UGIL 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 99.7% 1 <br /> Toluene-d8 77-150 SMEA 97.3% 1 <br /> W. ibromofluoromethane 57-156 SMEA 107.2% 1 <br /> • <br /> Approved by: Date: d U� <br />