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Alk <br /> ETelephone: <br /> 10 Second Avenu outh,##D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. 925-798-1620 Fax:925-798-1622 <br /> ' 1 E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Emil's Liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received: 01/30/99 <br /> Stockton, CA 95205 Client Contact: Gary Dickenson Date Extracted: 01/30-02/05199 <br /> CIient P.O: Date Analyzed: 02103-02/10/99 <br /> EPA analytical methods 6010/200.7,239,2* Lead* <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 02594 SB-1-11' S TTLC 4,7 107 <br /> 02597 SB-1-26.5' :� S TTLC ND 98 <br /> 02598 SB-1-31' S TTLC ND 101 <br /> i <br /> Reporting Limit unless otherwise S TTLC 3.0 mg/kg <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> --- STLC,TCLP 0.2 mg/L <br /> 'soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC/SPLP!TCLP extracts in mg/L <br /> *Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> °surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> &reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than —2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />