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r <br /> 110 Second Avenu uth,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax.925-798-1622 <br /> http://www.mccampbell.co!n E-mail. main@mccampbell.com <br /> i <br /> Advanced GeoEnvironmental Client Project ID: Emil's Liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received: 01/30/99 <br /> Stockton,CA 95205 Client Contact: Gary Dickenson Date Extracted: 02/01/99 <br /> —T— <br /> Client P.O: Date Analyzed: 02/02/99 <br /> LUFT Metals* <br /> rEPAn,71 ,,lmethods 6010/200.7,239.2' <br /> Lab ID Client ID Matrix Extraction' Cadmium Chromium Lead Nickel Zinc %Recovery <br /> Surrogate <br /> 02599 SP-7 S TTLC ND 16 6.7 12 54 100 <br /> 02600 SP-6 S TTLC ND 15 9.8 13 130 102 <br /> • <br /> Reporting Limit unless S TTLC 0.5 mg/kg 0.5 3.0 2.0 1.0 <br /> otherwise stated;ND <br /> means not detected above W TTLC 0.005 mg/L 0.005 0.005 0.05 0.05 <br /> the reporting limit _ STLC, <br /> TCLP 0.01 mg/L 0.05 0.2 0.05 0.05 <br /> "water samples are reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> "Lead is analysed using EPA method 6010(1CP)for soils,STLC&TCLP extracts and method 239.2(AA Furnace)for water samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(w2ter,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> "surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than —2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />