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1102nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax :925-798-1622 <br /> bUp://www.mccauMbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Emil's Liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received. 01/30/99 <br /> Stockton, CA 95205 Client Contact: Gary Dickenson Date Extracted: 02/02-02/05/99 <br /> Client P.O: Date Analyzed: 02/02-02105/99 <br /> Oxygenated Volatile Organics By GCT S <br /> EPA method 8260 modified <br /> Lab 1D 02594 02597 02598 <br /> Reporting Limit <br /> Client ID SB-1-1 1' SB-1-26.5' SB-1-31' <br /> Matrix S S S S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND NO NO 5.0 1.0 <br /> i <br /> i <br /> Ethyl tert-Butyl Ether(ETRE) ND NO NO 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) NO NO ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) NO t. NO NO 5.0 1.0 <br /> i <br /> tert-Butanol NO NO NO 25 5.0 <br /> i <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 106 100 101 <br /> Comments: <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> 1 <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />