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• I IQ 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax : 925-798-1622 <br /> hnp7//www.m;camj2bpJl.cE-mail:main@mccarnpbell.com <br /> Advanced GeoEnvironmental Client Project ID: Emil's Liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received: 01/30/99 <br /> Stockton, CA 95205 Client Contact: Gary Dickenson Date Extracted: 01/30-02/05/99 <br /> Client P.O: Date Analyzed: 02103-02110199 <br /> Lead* <br /> EPA analytical methods 6010/200.7,239.2* <br /> Lair ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 02594 SB-1-11' S TTLC 4.7 107 <br /> 02597 SS-1-26.5' S TTLC ND 98 <br /> 02598 SS-1-31' S TTLC ND 101 <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> -- STLC,TCLP 0.2 mg/L <br /> *soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC I SPLP I TCLP extracts in mg/L <br /> 'Lead is analysed using EPA method 6010 (1CP)fo7- soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water , <br /> samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> °surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> ° reporting limit raised due matrix interference <br /> 0 liquid sample that contains greater than --2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> Methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />