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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hap; lwww.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Emil's liquors Date Sampled: 01/28/99 <br /> 4005 North Wilson Way Date Received: 01/30/99 <br /> Stockton, CA 95205 Client Contact: Gary Dickenson Date Extracted: 02/01/99 <br /> Client P.O: Date Analyzed: 02/02/99 <br /> LUFT Metals* <br /> EPA analytical methods 6010/200.7,239.2' <br /> Lab 1D Client 1D Matrix Extraction' Cadmium Chromium Lead Nickel Zinc %Recovery <br /> Surrogate <br /> 02599 SP-7 S TTLC ND 16 6.7 12 54 100 <br /> 02600 SP-6 S TTLC ND 15 9.8 13 130 102 <br /> S TTLC 0.5 mg/kg 0.5 3.0 2.0 1.0 <br /> Reporting Limit unless <br /> otherwise stated;NO W TTLC 0.005 mg/L 0,005 0.005 0.05 0.05 <br /> means not detected above <br /> the reporting limit ___ STLC <br /> TCLP' 0.01 mg/L 0.05 0.2 0.05 0.05 <br /> 'water samples are reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in mg/L <br /> `Lead is analysed using EPA method 6010(ICP)for soils,STLC&TCLP extracts and method 239.2(AA Furnace)for water samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> "surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> &reporting limit raised due to matrix interference <br /> 0 liquid sample that contains greater than --2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> r <br /> DHS Certification No. 1644 l Edward Hamilton, Lab Director <br />