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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-20@10' <br /> Lab Sample ID: 720-1746-1 Date Sampled: 01/26/2006 1040 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 82608 Analysis Batch:720-5468 Instrument ID: Saturn 2100 <br /> Preparation: 50306-Medium Prep Batch: 720-5470 Lab File ID: c:\saturnwsklata\200602\02 <br /> Dilution: 200 Initial WeighWolume: 5.19 g <br /> Date Analyzed: 02/09/2006 2230 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 0,96 <br /> Benzene ND 096 <br /> Ethanol ND 96 <br /> Ethylbenzene 1.5 0.96 <br /> MTBE ND 0.96 <br /> TAME ND 0.96 <br /> Toluene ND 0.96 <br /> Xylenes,Total 10 1.9 <br /> TBA ND 1.9 <br /> DIPE ND 0.96 <br /> EDB ND 0.96 <br /> Gasoline Range Organics(GRO)-C6-C12 870 190 <br /> Ethyl tert-butyl ether ND 0.96 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 104 70- 130 <br /> 1,2-Dichloroethane-d4 99 60- 140 <br /> STL San Francisco Page 4 of 24 <br />