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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-20@15' <br /> Lab Sample ID: 720-1746-2 Date Sampled: 01/26/2006 1045 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 8260B Volatile Organic Compounds by GCIMS <br /> Method: 82608 Analysis Batch: 720-5468 Instrument ID: Saturn 2100 <br /> Preparation: 50308-Medium Prep Batch: 720-5470 Lab File ID: c:\saturnws\data\200602\02 <br /> Dilution: 400 Initial Weight/Volume: 5.21 g <br /> Date Analyzed: 02/09/2006 2256 Final Weight[Volume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 1.9 <br /> Benzene ND 1.9 <br /> Ethanol ND 190 <br /> Ethylbenzene 19 1.9 <br /> MTBE ND 1.9 <br /> TAME ND 1.9 <br /> Toluene ND 1.9 <br /> Xylenes,Total 99 3.8 <br /> TBA ND 3.8 <br /> DIPE ND 1.9 <br /> EDB ND 1.9 <br /> Gasoline Range Organics(GRO)-C6-C12 960 380 <br /> Ethyl tert-butyl ether ND 1.9 <br /> Surrogate %Rao Acceptance Limits <br /> Toluene-d8 87 70- 130 <br /> 1,2-Dichloroethane-d4 78 60- 140 <br /> STL San Francisco Page 5 Of 24 <br />