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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-20@30' <br /> Lab Sample ID: 720-1746-3 Date Sampled: 01/26/2006 1115 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 82606 Analysis Batch: 720-5465 Instrument ID: Saturn 39008 <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200602\02 <br /> Dilution: 1.0 Initial WeightA/olume: 5.09 g <br /> Date Analyzed: 02/09/2006 1258 Final WeighWolume: 10 mL <br /> Date Prepared: 02/09/2006 1258 <br /> Analyte DryM Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane NO 0.0049 <br /> Benzene ND 0.0049 <br /> Ethanol ND 0.49 <br /> Ethylbenzene NO 0.0049 <br /> MTBE NO 0.0049 <br /> TAME ND 0.0049 <br /> Toluene ND 0.0049 <br /> Xylenes, Total NO 0.0098 <br /> TBA NO 0.0098 <br /> DIPE ND 0.0049 <br /> EDB ND 0.0049 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 0.98 <br /> Ethyl tert-butyl ether NO 0.0049 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 100 70- 130 <br /> 1,2-Dichloroethane-d4 87 60- 140 <br /> STL San Francisco Page 6 of 24 <br />