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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-21@30' <br /> Lab Sample ID: 720-1746-7 Date Sampled: 01/27/2006 0925 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 82606 Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-5488 Instrument ID: Saturn 2100 <br /> Preparation: 50308 Lab File ID: c:\saturnws\data\200602\02 <br /> Dilution: 1.0 Initial Weight/Volume: 1.00 g <br /> Date Analyzed: 02/10/2006 2129 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/10/2006 2129 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 0.025 <br /> Benzene ND 0.025 <br /> Ethanol ND 2.5 <br /> Ethylbenzene ND 0.025 <br /> MTBE ND 0.025 <br /> TAME ND 0.025 <br /> Toluene ND 0.025 <br /> Xylenes, Total ND 0.050 <br /> TBA ND 0.050 <br /> DIPE ND 0.025 <br /> EDB ND 0.025 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 5.0 <br /> Ethyl tert-butyl ether ND 0.025 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 95 70- 130 <br /> 1,2-Dichloroethane-d4 95 60- 140 <br /> STL San Francisco Page 10 of 24 <br />