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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-21@40' <br /> Lab Sample ID: 720-1746-8 Date Sampled: 01/27/2006 0935 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 82608 Analysis Batch: 720-5465 Instrument ID: Saturn 3900B <br /> Preparation: 50308 Lab File ID: c:\saturnws\data\200602\02 <br /> Dilution: 1.0 Initial Weight/Volume: 5.04 g <br /> Date Analyzed: 02/09/2006 1559 Final WeightlVolume: 10 ml- <br /> Date <br /> LDate Prepared: 02/09/2006 1559 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 0.0050 <br /> Benzene ND 0.0050 <br /> Ethanol ND 0.50 <br /> Ethylbenzene 0.013 0.0050 <br /> MTBE ND 0.0050 <br /> TAME ND 0.0050 <br /> Toluene ND 0.0050 <br /> Xylenes, Total 0.048 0.0099 <br /> TBA ND 0.0099 <br /> DIPE ND 0.0050 <br /> EDB ND 0.0050 <br /> Gasoline Range Organics(GR0)-C6-C12 ND 0.99 <br /> Ethyl tert-butyl ether ND 0.0050 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 111 70- 130 <br /> 1,2-Dichloroethane-d4 82 60- 140 <br /> STL San Francisco Page 11 of 24 <br />