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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Client Sample ID: MW-21@46- <br /> Lab Sample ID: 720-1746-9 Date Sampled: 01/27/2006 0945 <br /> Client Matrix: Solid Date Received: 01/30/2006 0750 <br /> 82608 Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-5465 Instrument ID: Saturn 39008 <br /> Preparation: 50308 Lab File ID: c:\saturnws\data\200602\02 <br /> Dilution: 1.0 Initial Weight/Volume: 5.09 g <br /> Date Analyzed: 02/09/2006 1625 FinalWeight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1625 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane NO 0.0049 <br /> Benzene NO 0.0049 <br /> Ethanol NO 0.49 <br /> Ethylbenzene ND 0.0049 <br /> MTBE NO 0.0049 <br /> TAME NO 0.0049 <br /> Toluene NO 0.0049 <br /> Xylenes,Total NO 0.0098 <br /> TBA ND 0.0098 <br /> DIPE NO 0.0049 <br /> EDB NO 0.0049 <br /> Gasoline Range Organics(GRO)-C6-C12 NO 0.98 <br /> Ethyl tert-butyl ether NO 0.0049 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 104 70- 130 <br /> 1,2-Dichloroethane-d4 80 60- 140 <br /> STL San Francisco Page 12 of 24 <br />