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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Laboratory Control/ Method: 8260B <br /> Laboratory Control Duplicate Recovery Report-Batch: 720-5465 Preparation: 5030B <br /> LCS Lab Sample ID:LCS 720-5465/4 Analysis Batch: 720-5465 Instrument ID: Saturn 3900B <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 5 g <br /> Date Analyzed: 02/09/2006 1037 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1037 <br /> LCSD Lab Sample ID:LCSD 720-5465/3 Analysis Batch: 720-5465 Instrument ID: Saturn 3900B <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\02( <br /> Dilution: 1.0 Units:mg/Kg Initial Weight[Volume: 5 g <br /> Date Analyzed: 02/09/2006 1103 Final WeightA/olume: 10 mL <br /> Date Prepared: 02/09/2006 1103 <br /> %Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qua] <br /> Benzene 84 80 69-129 4 20 <br /> MTBE 79 84 65-165 5 20 <br /> Toluene 95 91 70-130 4 20 <br /> Surrogate LCS%Rec LCSD%Rec Acceptance Limits <br /> Toluene-d8 107 104 70- 130 <br /> 1,2-Dichloroethane-d4 74 77 60- 140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 18 of 24 <br />