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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Matrix Spike/ Method: 82608 <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-5465 Preparation: 5030B <br /> MS Lab Sample ID: 720-1746-3 Analysis Batch: 720-5465 Instrument ID: Saturn 3900B <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\I <br /> Dilution: 1.0 Initial Weight/Volume: 5.07 g <br /> Date Analyzed: 02/09/2006 1324 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1324 <br /> MSD Lab Sample ID: 720-1746-3 Analysis Batch: 720-5465 Instrument ID: Saturn 39008 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 1.0 Initial WeighWolume: 5.08 g <br /> Date Analyzed: 02/09/2006 1349 Final WeighWolume: 10 mL <br /> Date Prepared: 02/09/2006 1349 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Benzene 87 85 69- 129 2 20 <br /> MTBE 93 80 65-165 15 20 <br /> Toluene 92 96 70-130 5 20 <br /> Surrogate MS%Rec MSD% Rec Acceptance Limits <br /> Toluene-d8 101 102 70- 130 <br /> 1,2-Dichloroethane-d4 82 74 60-140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 19 of 24 <br />