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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Laboratory Control/ Method: 8260B <br /> Laboratory Control Duplicate Recovery Report-Batch: 720-5470 Preparation: 5030B <br /> LCS Lab Sample ID:LCS 720-5470/2-A Analysis Batch: 720-5468 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: 720-5470 Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 200 Units: mg/Kg Initial Weight/Volume: 5 g <br /> Date Analyzed: 02/09/2006 1639 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> LCSD Lab Sample ID:LCSD 720-5470/3-A Analysis Batch: 720-5468 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: 720-5470 Lab File ID: c:\saturnws\data\200602\02( <br /> Dilution: 200 Units:mg/Kg Initial Weight/Volume: 5 g <br /> Date Analyzed: 02/09/2006 1705 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> %Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Benzene 99 95 69- 129 3 20 <br /> MTBE 100 91 65-165 9 20 <br /> Toluene 104 98 70-130 6 20 <br /> Laboratory Control/ Method: 8260B <br /> Laboratory Control Duplicate Recovery Report-Batch: 720-5470 Preparation: 5030B <br /> LCS Lab Sample ID:LCS 720-5470/2-A Analysis Batch: 720-5468 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: 720-5470 Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 200 Units: ug/Kg Initial Weight/Volume: 5 g <br /> Date Analyzed: 02/09/2006 1639 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> LCSD Lab Sample ID:LCSD 720-5470/3-A Analysis Batch: 720-5468 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: 720-5470 Lab File ID: c:\saturnws\data\200602\02( <br /> Dilution: 200 Units:ug/Kg Initial WeightA/olume: 5 g <br /> Date Analyzed: 02/09/2006 1705 Final WeightfVolume: 10 mL <br /> Date Prepared: 02/09/2006 1500 <br /> Surrogate LCS%Rec LCSD%Rec Acceptance Limits <br /> Toluene-d8 105 104 70- 130 <br /> 1,2-Dichloroethane-d4 96 86 60- 140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 21 of 24 <br />