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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1746-1 <br /> Method Blank - Batch: 720-5488 Method: 82608 <br /> Preparation: 50308 <br /> Lab Sample ID: MB 720-5488/6 Analysis Batch: 720-5488 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: cAsaturnws\data\20060210: <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 5 g <br /> Date Analyzed: 02/10/2006 2037 Final WeighWolume: 10 mL <br /> Date Prepared: 02/102006 2037 <br /> Analyte Result Qual RL <br /> 1,2-Dichloroethane ND ^� 0.0050 <br /> Benzene ND <br /> 0.0050 <br /> Ethanol <br /> ND 0.50 <br /> Ethylbenzene ND 0.0050 <br /> MTBE ND 0.0050 <br /> TAME ND 0.0050 <br /> Toluene ND 0.0050 <br /> Xylenes,Total ND 0.010 <br /> TBA ND 0.010 <br /> DIPE ND 0.0050 <br /> EDB ND 0.0050 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 1.0 <br /> Ethyl tert-butyl ether ND 0.0050 <br /> Surrogate % Rec Acceptance Limits <br /> Toluene-d8 90 70- 130 <br /> 1,2-Dichloroethane-d4 90 60- 140 <br /> Laboratory Control Sample- Batch: 720-5488 Method: 8260B <br /> Preparation: 50308 <br /> Lab Sample ID: LCS 720-5488/5 Analysis Batch: 720-5488 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:lsaturnws\data\200602\0: <br /> Dilution: 1.0 Units:mg/Kg Initial WeighWolume: 5 g <br /> Date Analyzed: 02/10/2006 2010 Final WeighWolume: 10 mL <br /> Date Prepared: 02/10/2006 2010 <br /> Analyte Spike Amount Result %Rec. Limit oust <br /> Benzene 0.0500 0.046 92 69- 129 <br /> MTBE 0.0500 0.040 80 65- 165 <br /> Toluene 0.0501 0.044 87 70- 130 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 92 70- 130 <br /> 1,2-Dichloroethane-d4 84 60-140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 22 of 24 <br />