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.. <br /> Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1876-1 <br /> Client Sample ID: MW-20@65' <br /> Lab Sample ID: 720-1876-2 Date Sampled: 01/31/2006 1130 <br /> Client Matrix: Solid Date Received: 02/03/2006 0920 <br /> 82608 Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-5615 Instrument ID: Saturn 2100 <br /> Preparation: 50308 Lab File ID: c:\saturnws\data\20D602\02 <br /> Dilution: 1.0 Initial WeightlVolume: 5.15 g <br /> Date Analyzed: 02/14/2006 2320 FinalWeight/Volume: 10 mi- <br /> Date <br /> LDate Prepared: 02/14/2006 2320 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 4.9 <br /> Benzene ND 4.9 <br /> Ethanol ND 490 <br /> Ethylbenzene ND 4.9 <br /> MTBE ND 4.9 <br /> TAME ND 4.9 <br /> Toluene ND 4.9 <br /> Xylenes, Total ND 9.7 <br /> TBA ND 9.7 <br /> DIPE ND 4.9 <br /> EDB ND 4.9 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 970 <br /> Ethyl tert-butyl ether ND 4.9 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 97 70-130 <br /> 1,2-Dichloroethane-d4 96 60-140 <br /> STL San Francisco Page 5 Of 16 <br />