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Analytical Data <br /> Client: Secor International, Inc. Job Number: 720-1876-1 <br /> Client Sample ID: MW-20@70' <br /> Lab Sample ID: 720-1876-3 Date Sampled: 01/31/2006 1135 <br /> Client Matrix: Solid Date Received: 02/03/2006 0920 <br /> 82608 Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch:720-5615 Instrument ID: Saturn 2100 <br /> Preparation: 50306 Lab File ID: c:\saturnwMdata\200602\02 <br /> Dilution: 1.0 Initial Weight(Volume: 5.1 g <br /> Date Analyzed: 02/14/2006 2346 Final Weight(Volume: 10 mL <br /> Date Prepared: 02/14/2006 2346 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier <br /> 1,2-Dichloroethane ND 4.9 <br /> Benzene ND 4.9 <br /> Ethanol ND 490 <br /> Ethylbenzene 5.7 4.9 <br /> MTBE NO 4.9 <br /> TAME ND 4.9 <br /> Toluene ND 4.9 <br /> Xylenes,Total 28 9.8 <br /> TBA NO 9.8 <br /> DIPE ND 4.9 <br /> EDB ND 4.9 <br /> Gasoline Range Organics(GRO)-C6-C12 NO 980 <br /> Ethyl tert-butyl ether ND 4.9 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 98 70- 130 ^� <br /> 1,2-Dichloroethane-d4 100 60- 140 <br /> STL San Francisco Page 6 of 16 <br />