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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1876-1 <br /> Laboratory Control/ Method: 8260B <br /> Laboratory Control Duplicate Recovery Report-Batch: 720-5615 Preparation: 5030B <br /> LCS Lab Sample ID:LCS 720-5615/9 Analysis Batch: 720-5615 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 1.0 Units: ug/Kg Initial WeighUVolume: 5 g <br /> Date Analyzed: 02/14/2006 2109 Final WeighWolume: 10 mL <br /> Date Prepared: 02/14/2006 2109 <br /> LCSD Lab Sample ID:LCSD 720-5615/3 Analysis Batch: 720-5615 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\021 <br /> Dilution: 1.0 Units:ug/Kg Initial WeighWolume: 5 g <br /> Date Analyzed: 02/14/2006 2201 Final WeighWolume: 10 mL <br /> Date Prepared: 02/14/2006 2201 <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Dual LCSD Qual <br /> Benzene 114 115 69- 129 1 20 <br /> MTBE 110 114 65- 165 4 20 <br /> Toluene 114 113 70- 130 1 20 <br /> Surrogate LCS% Rec LCSD% Rec Acceptance Limits <br /> Toluene-d8 96 97 70- 130 <br /> 1,2-Dichloroethane-d4 89 91 60- 140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 10 of 16 <br />