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Quality Control Results <br /> Client: Secor International, Inc. Job Number: 720-1876-1 <br /> Matrix Spike/ Method: 8260B <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-5615 Preparation: 5030B <br /> MS Lab Sample ID: 720-1839-A-5 MS Analysis Batch: 720-5615 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\I <br /> Dilution: 1.0 Initial Weight/Volume: 5.08 g <br /> Date Analyzed: 02/15/20060132 Final WeighWolume: 10 mL <br /> Date Prepared: 02/15/2006 0132 <br /> MSD Lab Sample ID: 720-1839-A-5 MSD Analysis Batch: 720-5615 Instrument ID: Saturn 2100 <br /> Client Matrix: Solid Prep Batch: N/A Lab File ID: c:\saturnws\data\200602\0: <br /> Dilution: 1.0 Initial WeighWolume: 5.07 g <br /> Date Analyzed: 02/15/2006 0158 Final WeightA/olume: 10 mL <br /> Date Prepared: 02/15/2006 0158 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Benzene 92 99 69-129 8 20 <br /> MTBE 90 101 65-165 12 20 <br /> Toluene 90 100 70-130 11 20 <br /> Surrogate MS%Rec MSD%Rec Acceptance Limits <br /> Toluene-d8 91 95 70-130 <br /> 1,2-Dichloroethane-d4 90 91 60-140 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 11 of 16 <br />