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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fa z 925-798 1622 <br /> http llwww ince bell coin E mmil main ca bell coin <br /> Advanced GeoEnvirorunental,Inc Client Project ID Flag City Chevron Date Sampled 12/09/03 <br /> 837 Shaw Road Date Received 12/10/03 <br /> Client Contact Ton Cuellar Date Extracted 12/10/03 <br /> Stockton, CA 95215 <br /> [Client P Q Date Analyzed 12/10/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> ExtaactuonMethod SW5030B Analytical Method SW8260B Work Order 0312187 <br /> Lab ID 0312187-017C 0312187-018C I <br /> I <br /> Client ID Influent Effluent <br /> i Reporting Limit for <br /> Matrix W W I DF=1 <br /> —---- --- -------- — <br /> DF 1 1 S W <br /> Compound Concentration ug/kg 14 L <br /> Cert-Amyl methyl ether(TAME) ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND NA 05 <br /> 12-Dichloroethane(1,2-DCA) ND ND NA 05 <br /> Dusopropyl ether(DIPE) ND ND NA 05 <br /> Ethanol ND ND NA 50 <br /> Ethyl tert-butyl ether(ETRE) ND ND NA 05 <br /> Methanol ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) 20 ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 106 106 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soiVsludge/solid samples in ug/kg, wipe samples in jig/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,,/)sample diluted due to high <br /> or anic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />