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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> 4 McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> Nip//www mccampbcll corn E-mail main mccampbell corn <br /> Advanced GeoEnvrronmental,Inc Client Project ID Flag City Chevron Date Sampled 12/09/03 <br /> 837 Shaw Road Date Received 12/10/03 <br /> Stockton,CA 95215 Client Contact Tun Cuellar Date Extracted 12/10/03 <br /> Client P O Date Analyzed 12/10/03 <br /> Lead by Graphite Furnace Atomic Absorption* <br /> Extraction method E200 9 Analytical methods F200 9 Work Order 0312187 <br /> Lab ID Client ID Matrix Extraction Lead DF %SS <br /> 0312187-017D Influent W TTLC ND I NIA <br /> E <br /> Reporting Limit for DF=1, W TTLC 0 005 rng/L <br /> ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> *water/product/oillnon-aqueous liquid samples and ail TCLP I STLC/DISTLC I SPLP extracts are reported to mg/L soil/sludge/solid samples in mg/kg, <br /> wipe samples in gg/wipe filter samples inµg/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference &means low or no surrogate due to matrix interference,ND means not <br /> detected above the reporting limit,NIA means not applicable to this sample or instrument <br /> Analytical Methods EPA 60100/200 7 for all elements except 200 9(water/liquid-Sb As,Pb Se,TI),245 l (Hg),7010 <br /> (sludge/soil/solid/oti/producdwipe/filter-As,Se,Tl),747IB(Hg) <br /> i)liquid sample that contains greater than—2 vol %sediment this sediment is extracted with the liquid in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting Iimit raised due to insufficient sample amount,k)results are reported by dry weight y) <br /> estimated values due to low surrogate recovery,z)reporting limit raised due to matrix interference <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />