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1102nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925 798-1622 <br /> h 1 <br /> /www mccampbel!coin E-mail mom mccampbell eom <br /> Advanced GeoEnvironinental,Inc Client Project ID Flag City Chevron Date Sampled 11/19/03 <br /> 837 Shaw Road Date Received 11/20/03 <br /> Client Contact Tun Cuellar Date Extracted 11/21/03 <br /> Stockton,CA 95215 <br /> Client P O 1 Date Analyzed 11/21/03 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0311268 <br /> Lab ID 0311268-003A 0311268-004A i 0311268-005A <br /> 3 <br /> Client ID GAC-1 GAC-2 SS-1 <br /> Reporting Limit for <br /> Matrix W W W DF=1 <br /> i E <br /> Compound Concentration ug/kg µg/L <br /> tent-Amyl methyl ether(TAME) ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND NA 50 <br /> Dnsopropyl ether(DIPE) ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBF) ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) 18 11 ND NA 05 <br /> Surrogate Recoveries (%) <br /> %SS 105 105 111 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L soiUsludgelsolid samples in lig/kg, wipe samples in jig/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out ofrange or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br />