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110 2nd Avenue South #D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-799-1620 Fax 925-798-1622 Z—A-- <br /> http Ilwww mccan bell corn E mail rmin@rriccarnplyell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 11/19/03 <br /> 837 Shaw Road Date Received 11/20/03 <br /> Client Contact Tum Cuellar Date Extracted 11/21/03 <br /> Stockton,CA 95215 <br /> [Client P O Date Analyzed 11/21/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0311268 <br /> Lab ID 0311268-001C 0311268-0020 <br /> Client ID Influent Effluent <br /> � Reporting Limit for <br /> Matrix W W ; DF=1 <br /> DF I S W <br /> Compound Concentration ug/kg gg/L <br /> tert-Amyl methyl ether(TAME) ND NI) NA 05 <br /> t-Butyl alcohol(TBA) ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND NA 05 <br /> 1,2-Dtchloroethane(1,2-DCA) ND ND NA 05 <br /> Dnsopropyl ether(DIPE) ND ND NA 05 <br /> Ethanol ND ND NA 50 <br /> Ethyl tent-butyl ether(ETBE) ND ND NA 05 <br /> E <br /> Methanol ND ND NA 500 <br /> Metbyl-t-butyl ether(MTBE) 27 ND NA 05 <br /> Tetrachloroethene ND ND NA 05 <br /> Trichloroethene ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 104 107 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in gg/kg, wipe samples in gg/wipe, <br /> product oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> 11 surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,3)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />