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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> McCainphell Analytical Inc Telephone 925-798 1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main mccampbell corn <br /> • Advanced GeoEnvironmental,Inc Client Project ID FIag City Chevron Date Sampled 11/19/03 <br /> 837 Shaw Road Date Received 11/20/03 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 11/20/03 <br /> Client P O Date Analyzed 11/20/03 <br /> Lead by Graphite Furnace Atomic Absorption* <br /> Extraction method E200 9 Analytical methods E200 9 Work Order 0311268 <br /> Lab ID Client ID Matrix Extraction Lead DF %SS <br /> 0311268-001 D Influent W TTLC ND 1 N/A <br /> Reporting Limit for DF=1, W TTLC 0 005 mg/L <br /> ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> 'water/produU/oiVnon-aqueous liquid samples and all TCLP 1 STLC/DISTLC/SPLP extracts are reported in mg/L,sotUsludge/solid samples to mg/kg, <br /> wipe samples in jig/wipe,filter samples inµg/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference,&means low or no surrogate due to matrix interference,ND means not <br /> detected above the reporting limit,N/A means not applicable to this sample or instrument <br /> Analytical Methods EPA 6016C/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se,T1),245 1 (Hg) 7010 <br /> (sludge/soil/solid/oil/product/wipelfilter-As,Se,TI),7471B(Hg) <br /> i)liquid sample that contains greater than--2 vol %sediment,this sediment is extracted with the liquid,to accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting limit raised due to insufficient sample amount,k)results are reported by dry weight,y) <br /> estimated values due to low surrogate recovery,z)reporting limit raised due to matrix interference <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />