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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> - httpJ/www razz belLcom E-mail MK222EcIEEbell com <br /> Advanced GeoEnvironmental,Inc Client Project ID Three B's Date Sampled 06/25/03-06/26/03 <br />' 837 Shaw Road Date Received 06/27/03 <br /> Client Contact Tun Cuellar Date Extracted 07/02/03-07/03103 <br /> Stockton, CA 95215 <br />' CIient P O Date Analyzed 07/02/03-07/03/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method.SW8260B Work Order 0306602 <br /> Lab ID 0306602-009B 0306602-01 OB 0306602-0118 0306602-012B <br /> Client ID MW10b MW1Oa MW9a MW9b <br /> Reporting Limit for <br /> Matrix W W W W DP=1 <br /> _ 1 , <br /> DF 1 33 i 1 i 1 S W <br /> ICompound Concentration ug/kg µg/1. <br /> tert-Amyl methyl ether(TAME) ND ND<17 ND ND NA 05 <br /> IBenzene 33 620 1 0 062 NA 05 <br /> t-Butyl alcohol(TBA) ND ND<170 ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND<17 ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND<17 ND ND NA 05 <br /> Dusopropyi ether(DIPE) ND ND<17 ND ND NA 05 <br /> Ethylbenzene ND ND<l7 ND ND NA 05 <br /> Ethyl tent-butyl ether(F-TBE) ND ND<17 ND ND NA 0 5 <br /> IMethyl-t-butyl ether(MTBE) 12 ND<17 ND ND NA 05 <br /> Toluene ND ND<17 ND ND NA 05 <br /> IXylenes ND ND<17 ND ND NA 05 <br /> Surrogate Recovenes(%) <br /> I0%SS1 109 104 110 110 <br /> I %SS2 999 101 101 100 <br /> %SS3 111 115 113 114 <br /> IComments i <br /> water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/ofton-aqueous liquid samples in mg/L- <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> or is content <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />