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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> F4 McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br />' h !/www nwcanipbcil com E-mad niani@nweangbell com <br /> . Advanced GeoEnvironmental, Inc Chent Project ID Three B's Date Sampled 06/25/03-06/26/03 <br />' 837 Shaw Road Date Received 06/27/03 <br /> Stockton,CA 95215 Chent Contact Tun Cuellar Date Extracted 07/02/03-07/03/03 <br />' Client P O Date Analyzed 07102/03-07/03/03 <br /> Oxygenates and BTEX by GC/MS* <br />' Exlr"Uon Method.5W511308 Anaiyucal Meflod.SW8260B Work Order 0306602 <br /> Lab ID 0306602-005B 10306602-006B 0306602-007B 1 0306602-OOSB <br /> i <br /> Client YD MW10f MW10e i MW10d MW10c Reporting Limit for <br />' Matrix W I W W W DF=1 <br /> I <br /> DF 1 I 1 1 S W <br />' Compound Concentration ug/kg µell <br /> tent-Amyl methyi ether(TAME) ND ND ND ND NA 05 <br />' Benzene 088 070 058 63 NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND AIA 50 <br />' 1,2-Dibmmoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br />'. Dusopropyl ether(DiPE) ND ND ND ND [--�NA 05 <br /> Ethylbcnzene ND ND ND ND NA 05 <br /> Ethyl Cert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND 1 1 NA 05 <br /> Toluene ND ND ND ND NA 05 <br /> Xylenes ND ND ND ND NA I 05 <br /> Surrogate Recovenes{%) <br /> %SSI 109 108 107 109 <br /> %SS2 997 100 100 979 <br /> %SS3 105 104 105 113 <br /> Comments <br /> — I T:---7 <br /> *water and vapor samples and all TCLP&SPLF extracts are reported inµgll. soil/sludge/solid samples inµg/kg, wipe samples in}tg/vnpc, <br /> product/o11/non-aqueous liquid samples m mg"— <br /> ND means not detected above the reporting Itmit,N/A means analyte not applicable to this analysis <br /> #sumPte di luted out of range or surrogate coelutes with another peals <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS CeTtitcation No 1644 Angela Rydehus,Lab Manager <br />