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I <br /> 110 2nd Avenue South,#1)7 Pacheco CA 94553 5560 <br /> _ MCCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> httpJ/www mccamphell com E-mad =m@mccLnTbellcom <br /> Advanced GeoEnvlronmental,Inc Client Project ID Three B's Date Sampled 06/25/03-06/26103 <br /> 837 Shaw Road Date Received 06/27/03 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 07/02/03-07/03103 <br /> [Client P O Date Analyzed 07/02/03-07/03103 <br /> Oxygenates and BTEX by GC/MS* <br /> I Es1372e1wn Method SWI03013 Analytical Method.SW8260B Work Order 0306602 <br /> Lab ID 0306602-001B 0306602-0021 0306602-0038 0306602-0048 <br /> Client ID MW4 ` MW5 i MWl 1 e I MWI if Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF 25 1 1 1 S W <br /> ICompound Concentration ug/kg Ag/L <br /> tert-Amyl methyl ether(TAME) ND<2 ND ND ND NA 05 <br /> IBenzene ND<I 2 5 7 ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND<12 4 8 ND ND NA 5 0 <br /> 1,2-Dibtnmoethane(EDB) ND<l 2 ND ND ND NA 05 <br /> 1,2-Drchloroethane(1,2-DCA) ND<l 2 ND ND ND NA Q 5 <br /> Dusopropyl ether(DIPS) ND<1 2 ND ND ND NA 010 <br /> 5 <br /> Ethylbenzene ND<1 2 ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETRE) ND<I 2 ND ND ND NA Q 5 <br /> Methyl-t-butyl ether(MTBE) 70 ND ND ND NA 05 <br /> Toluene ND<1 2 ND ND ND NA 05 <br /> Xylenes ND<i 2 ND ND ND NA 0 5 <br /> Surrogate Recoveries(%} <br /> %SSI 106 106 107 109 <br /> %SS2 985 972 985 98 1 <br /> %SS3 104 106 106 106 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported In gg/L,sotllsludgc/sohd samples mµg/kg, wipe samples 1n gg/wtpe, <br /> product/otl/non-aqueous liquid samples 1n mg/L. <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peals <br /> h)lighter than water Immiscible sheen/product Is present,1)liquid sample that contains greater than 2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />