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k <br /> 1102nd Avenue South,#137 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> b //www mccainpbell com E-mail niain@niccaMbell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 06/25/03 <br /> 837 Shaw Road Date Received 06/26/03 <br /> Client Contact Tim Cuellar Date Extracted 07/01/03-07/02/03 <br /> Stockton,CA 95215 <br />' Client P O Date Analyzed 07/01/03-07/02/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analybcal Method SW9260B Work Order 0306568 <br />' Lab ID 0306568-005B 0306568-006B 0306568-007B 0306568-008B <br /> Client ID MW6A MW6B MW7 MW16 <br /> Reporting Limit for <br />' Matrix W W W ,W DF=t <br /> DF ---I ---- —i —i 25 F S W <br />' Compound :E <br /> Concentration ug/kg Ili <br /> tert-Amyl methyl ether(TAME) ND ND ND ND<l 2 NA 05 <br />' Benzene ND ND ND ND<l 2 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND<12 NA 5 0 <br />' Ditsopropyl ether(DIPE) ND ND ND ND<l 2 NA 05 <br /> Ethanol ND ND ND ND<120 NA 50 <br />' • Ethylbenzene ND ND ND ND<1 2 NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND<1 2 NA 0 5 <br /> Methanol ND ND ND ND<1200 NA 500 <br /> Methyl-t-butyl ether(MTBE) ND 058 ND 79 NA 05 <br /> Toluene ND ND ND ND<1 2 NA 05 <br />' Xylenes ND ND ND ND<l 2 NA 0 5 <br /> Surrogate Recoveries(%) <br />' %SS1 102 101 105 107 <br />' %SS2 993 967 967 978 <br /> %SS3 975 972 978 950 <br /> Comments t <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples inµglkg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,1)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> • l organic content <br /> 1 <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />