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M 1D 2nd inue SouOi #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telepe 925-798-1620 Fax 925-798-1622 <br /> h Jhvww ampbeli com E maiE maar rnccair�belLcom <br /> EAA <br /> i Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 06/25/03 <br /> 837 Shaw Road Date Received 06/26/03 <br /> Client Contact Tim Cuellar Date Extracted 07/01/03-07/02/03 <br /> Stockton,CA 95215 <br />' r0ie�nPO Date Analyzed 07/01103-07/02/03 <br /> Oxygenates and BTEX by GC/MS* <br />' Extraction Method SW5030B Analytical Method SW8260B Work Order 0306568 <br /> Lab ID 0306568-009B 0306568-OIOB 0306568-OIIB 0306568-012B <br /> Client ID EW1 EW2 EW3 EW4 <br />' Reporting Limit for <br /> Matrix W W W W DF=1 <br />' Compound Concentration ug/kg lige <br />' tert-Amyl methyl ether(TAME) ND ND ND ND NA 01 <br /> Benzene ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br />' Dusopropyl ether(DIPS) ND ND ND ND NA 05 <br /> Ethanol ND ND ND ND NA 50 <br />' Ethylbenzene ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methanol ND ND ND ND NA 500 <br /> Methyl-t-butyi ether(MTBE) 056 12 ND 26 NA 05 <br /> Toluene ND ND ND ND NA 05 <br /> Xylenes ND ND ND ND NA 05 <br />' Surrogate Recoveries(%) <br /> %SSI 103 104 100 100 <br />' %SS2 970 972 956 972 <br /> %SS3 968 949 970 966 <br /> Comments <br /> water and vapor samples and all TCLP&SPLP extracts are reported in gg/L soil/sludge/solid samples in pg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means anaiyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> 1 h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than—2 vol %sediment, sample diluted due to high <br /> organic content <br />' DHS Certification No 1644 _ Angela Rydehus,Lab Manager <br />