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110 2nd Avenue South ND7 Pacheco,CA 94553 5560 <br /> McCarnpbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h J/www mcc bell com E-mad main mcca bell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 06/26/03 <br /> 837 Shaw Road Date Received 06/27/03 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 07/02/03-07/03/03 <br /> Client P O Date Analyzed 07/02/03-07/03/03 <br /> Oxygenates and BTEX by GC1MS* <br /> Extraction Method SW5030B Analytrcal Method SW8260B Work Order 0306601 <br />' Lab ID 0306601-001B 0306601-002B 0306601-003B 0306601-004B <br /> f � <br /> Client ID MW15 MW14 MW18 MW17 <br />' Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF --- 1 ---- 1 �--- 5 --�---5_ <br /> S W <br />' Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND<2 5 ND<2 5 NA 05 <br /> Benzene- ND ND ND<2 5 ND<2 5 NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND<25 ND<25 NA 50 <br />' Diisopropyl ether(DIPE) ND ND ND<2 5 ND<2 5 NA 0 5 <br /> Ethanol ND ND ND<250 ND<250 NA 50 <br /> Ethylbenzene ND ND ND<2 5 ND<2 5 NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND<2 5 ND<2 5 NA 0 5 <br /> Methanol ND ND ND<2500 ND<2500 ANA <br /> Methyl-t-butyl ether(MTBE) 60 ND 140 140 <br /> Toluene ND ND ND<2 5 ND<2 5 <br /> Xylenes ND ND ND<2 5 ND<2 5 <br /> Surrogate Recoveries(%) <br /> %SSI 101 102 104 107 <br /> %SS2 98 7 978 985 960 <br /> %SS3 961 965 987 983 <br /> IComments <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soillsludge/solid samples in ug/kg, wipe samples in jig/wipe, <br /> productlotl/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means anaiyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644Angela Rydelius, Lab Manager <br />