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110 2nd Avenue South #D7,Pacheco CA 94553-5560 <br /> 'telephone 925 798-1620 Fax 925-798-1622 <br /> McCampbell Analytical Inc <br />' http//www"canipbell com E mail =m@niccanipbell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 06/26/03 <br />' 837 Shaw Road Date Received 06/27/03 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 07102103-07/03/03 <br /> tClient P O Date Analyzed 07/02/03-07103/03 <br /> Oxygenates and BTEX by GC/MS* <br />' Extraction Method, SW51131111 Analytical Method.SW8260B Work Order 0306601 <br /> Lab 1D 0306601-005B 0306601-006B i 0306601-007B E 0306601-008B <br /> f <br /> Client ID MWIOb MWI0C I MW10d f MWl0e Reporting Limit for <br />' Matrix W W W W DF=1 <br /> DFS W <br /> 11 <br />' Compound Concentration Ug/kg µ... = .' ..I <br /> g/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br />' Benzene ND ND ND ND NA 0 5 <br /> t-Butyl alcohol(TSA) ND ND ND ND NA 5 0 <br />' Dusopropyl ether(DIPE) ND ND ND ND NA 05 <br /> Ethanol ND ND ND ND NA 50 <br />' Ethylbenzene ND ND ND ND NA 0 5 <br /> Ethyl ten-butyl ether(ETBE) ND ND ND ND NA 0 5 <br /> Methanol ND ND ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND ENA <br /> 0 5 <br /> Toluene ND ND ND ND 0 5 <br /> Xylenes ND ND ND ND NA 0 5 <br />' Surrogate Recoveries(%) <br /> %SSI 108 104 105 107 <br /> I %SS2 98 9 98 7 98 8 99 2 <br /> %SS3 979 98 2 983 98 6 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,sotllsludge/soltd samples toµg/kg, wipe samples to jig/wipe, <br /> product/oil/non-aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> I <br /> DHS Certification No 1644 '-_- Angela Rydelius, Lab Manager <br />