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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> J4 http//www mccampbelI corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID .Flag City <br /> Date Sampled 03/27-03128102 <br /> 837 Shaw Road Date Received 03/28/02 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 04/01/02 <br /> Client P O =DateAnalyzed 04/01/02 <br /> Volatile Organics By GUMS 4 <br /> EPA method 8260 <br /> Lab ID 0203513-035 <br /> Client ID EFFLUENT <br /> Matrix W <br /> Compound Concentration* RW� <br /> Limit Compound Concentration* Reporting Limit <br /> S W S <br /> Acetone ib1 ND 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromide J ND 10 50 <br /> Bromobenzene ND to 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 5 0 <br /> Bromoform ND 10 50 Isopropyl benzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride"' ND 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 l0 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone'g' ND 10 50 <br /> Cai bon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) ND 10 50 <br /> • Chlorobenzene ND 10 50 Naphthalene ND 50 50 <br /> Chloroethane ND<3 0 1 0 50 n-Propyl benzene AID 1 0 50 <br /> 2-Chloroetliyl Vinyl Ether` ND 10 50 _Styrene' ND 10 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Cliloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlolotoluene ND 1 0 50 Tetrachloroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 10 'o <br /> 050 Toluene ND 1 0 5 0 <br /> DibrOmochloromethane ND 1 0 50 1,2 3-Tnchlorobenzene ND 5 0 25 <br /> 1 2-DlbrOmo-3-chloropropane ND 20 10 1,2,4-Trichlorobenzene ND 50 25 <br /> Dibromomethane ND to 5 0 1,1,1-Trichloroethane ND to 5 0 <br /> 1,2-Diehlorabenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1 3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND j 1 0 50 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 1 0 50 <br /> 1,l-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> T,2-Dichloroethane ND 10 5 0 1,3,5-Tnrnethylbenzene ND 1 0 50 <br /> 10-Dichloroethene ND 1 0 50 Vinyl Acetate °' ND 5 0 25 <br /> c15-1,2-Dichloroethene ND 10 50 Vinyl Chloride ND 1 0 50 <br /> trans-1 2-Dichloroethene ND 1 0 50 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dicliloropropane ND to 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibrornofluoromethane 101 <br /> l,I-Dichloroptopene ND 10 50 Toluene-dg 97 <br /> c15-1 3-Dichloropropene ND _LLL 5 O 4-13romotluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroetboxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is piesent, (i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) metbYlbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 A Edward Hamilton, Lab Director <br />