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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCarnpbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com Email main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 04/02/02 <br />. 837 Shaw Road Date Received 04/04/02 <br /> Client Contact Tim Cuellar Date Extracted 04/11/02 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 04/11/02 <br /> Volatiles Organics by GCIMS(Basic Analyte List) <br /> Exuaetion Method SW5030B Analytical Method SW9260B Work Order 0204071 <br /> _ Lab ID 0204071-OOIA <br /> Client ID EFFLUENT <br /> Matnx Water <br /> Compound I Concentration* DF `Limit s Compound Concentration* DF I `� `;�& <br /> Acrolem(Propenal) ND 1 0 5 Acrylomtnle ND 1 0 2 <br /> Benzene ND 1 0 0 5 Bromodichlommethane ND 1 1 0 0 5 <br /> Bromoform ND 1 0 2 Bromomethane ND 10 2 <br /> Carbon Tetrachloride ND 1 0 0 5 Chlorobenzene ND 1 0 2 <br /> Chloroethane 1 ND 1 0 2 2-Chloroethyl Vinyl Ether ND 1 0 1 <br /> Chloroform I ND 1 0 1 0 5 Chloromethane ND 1 0 2 <br /> Dibromochloromethane ND 1 0 0 5 1,2-Dichlorobenzene ND 1 0 I 2 <br /> 1 3-Dichlorobenzene j ND 1 0 2 1 4-Dichlorobenzene ND 1 0 2 <br /> 1,1-Dichloroethane ND 1 1 0 1 1,2-Dichloroethane ND 1 0 0 5 <br /> 1 1-DichlOTDethene ND 1 0 0 5 cis-1,2-Dichloroethene ND 1 0 0 5 <br /> trans-1,2-Dichloroethene ND 1 0 1 1,2-Dichloropropane I ND 1 0 0 5 <br /> 1 3-Dichloropropane ND 1 0 0 5 Ethyl benzene ND 1 0 2 <br /> Hexachlorobutadlene ND 1 0 1 Hexachloroethane ND 1 1 0 I 1 <br /> Methyl-t-butyl ether(MTBE) ND 1 0 3 Methylene chloride ND 1 0 1 2 <br /> Naphthalene ND 1 0 10 Styrene ND 1 0 0 5 <br /> . 1 1 2,2-Tetrachloroethane ND 1 0 0 5 ? Tetrachloroethene ND 1 0 0 5 <br /> Toluene ND 1 0 2 1,2,4-Tnchlorobeozene ND 1 1 0 5 <br /> I,1 1-Trichloroethane j ND 1 0 2 1,1 2-Trichloroethane ND 1 0 0 5 <br /> Trichloroethene I ND 1 0 I 2 Trichlorofluoromethane ND 1 0 5 <br /> 1 1,2-Tnchloro-I,2,2-Tnfluoroethan ND 1 0 10 Vinyl Chloride ND 1 1 0 0 5 <br /> Xylenes ND 1 0 0 5 <br /> Surrogate Recoveries(%) <br /> Surr 4-Bromoflurobenzene 105 Surr Dibromofluoiomethane 975 <br /> Surr Toluene-d8 97 7 <br /> Comments <br /> *water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone,(c)(2-chloroethoxy)ethene (d)2-hexanone (e)dichloromethane,(f)2-butanone,(g)4-methyl-2-pentanone or <br /> isopropylacetone,(h)liglitei than water immiscible sheen/product is present (i)liquid sample that contains greater than—2 vol %sediment,0)sample <br /> diluted due to high oigame content (k)ethenylbenzene,(1)metbylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />