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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hap//www mccampbell conn E-mail mainQa mccampbell corn <br /> Advanced GcoEnvironmental Client Project ID Flag City Cheveron Date Sampled 03131/02&04102/02 <br /> 837 Shaw Road Date Received 04101102&04/03/02 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 04/03/02 <br /> Client P O Date Analyzed 04/05/02 <br /> Polynuclear Aromatic Hydrocarbons(PAH/PNA)by GC-MS <br /> EPA methods 625(modified 610)and 3510 or 8310(modified 8100)and 3550 <br /> Lab 1D 02040 00171 Reporting Limit <br /> Client 1D EFFLUENT w,STLC <br /> S <br /> Matrix W TCLP <br /> Compound Concentration* mg/kg ug/L <br /> Acenaphthene ND 0 062 1 <br /> Acenaphthylne ND 0 062 10 <br /> Anthracene ND 0 062 10 <br /> Benzo(a)anthracene ND 0 062 5 <br /> Benzo(b)fluoranthene ND 0 062 10 <br /> • Benzo(k)fluoranthene ND 0 062 2 <br /> Benzo(g,h,i)perylene, ND 0 062 5 <br /> Benzo(a)pyrene ND 0 062 2 <br /> Chrysene ND 0 062 5 <br /> Dibenzo(a,h)anthracene ND 0 062 01 <br /> Fluoranthene ND 0 062 10 <br /> Fluorene ND 0 062 10 <br /> 1ndeno(1,2,3-cd)pyrene ND 0 062 0 05 <br /> Naphthalene --- 0 062 10 <br /> Phenanthrene ND 0 062 5 <br /> Pyrene ND 0 062 10 <br /> %Recovery Surrogate 1 112 <br /> %Recovery Surrogate 2 121 <br /> Comments <br /> "water and vapor samples are reported in ug/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts to <br /> ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> "surrogate diluted out of range or surrogate coelutes with another peak <br /> • (h)a lighter than water immiscible sheen is present,(i)liquid sample that contains>-5 vb] %sediment, 0)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />