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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccTnbeE]com E-mail main@mccampbell corn <br />• <br /> Advanced GeoEnvironinental Client Project ID Flag City Cheveron Date Sampled 03131/02&04102/02 <br /> 837 Shaw Road Date Received 04101/02&04/03/02 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 04/03/02 <br /> Client P Q Date Analyzed 04108-04/10102 <br /> Semi-Volatile Organics By GC/MS <br /> EPA method 625 and 3510 or 8270 and 3550 <br /> Lab ID 0204071-001 <br /> Client ID EFFLUENT <br /> Matrix W <br /> Reporting Limit Reporting Limit <br /> Compound Concentration* Compound oncentration <br /> W S W S <br /> Acenaphthene — 10 0 33 Di-n-octyl Phthalate ND 10 033 <br /> Acenaphthylene -- 10 033 1,2-Diphenylhydrazme ND 1 033 <br /> Anthracene -- 10 033 Fluorantbene -- 10 033 <br /> Benzidine ND 5 1 6 Fluorene --- 10 033 <br /> Benzoic Acid --- 50 1 6 Hexachlorobenzene --- 10 033 <br /> Benzo(a)anthracene --- 10 033 Hexachlorobutadiene --- 10 033 <br /> Benzo(b)fluoranthene --- IO 033 Hexachlorocyclopentadiene ND 5 16 <br /> Benzo(k)fluoranthene -- 10 033 Hexachloroethane - 10 033 <br /> Benzo(g,bo)perylene - 10 033 Indeno(1,2,3-cd)pyrene -- 10 033 <br /> Benzo(a)pyrene 10 033 Isophorone ND 1 033 <br /> Benzyl Alcohol -- 20 066 2-Methylnaphthalene - 10 033 <br /> • Bis(2-chloroethoxy)methane ND 5 033 2-Methylphenol(o-Cresol) 10 033 <br /> Bis(2�hlomethyl)Ether ND 1 033 3 Wor 4-Methylphenol(m&Jar p-Cresol) 10 033 <br /> Bis(2-chloroisopropyl) ther ND 10 0 33 Naphthalene 10 033 <br /> Bis(2-ethythexyl)Phthalate ND 5 033 2-Nitroaniline --- 50 1 6 <br /> 4-Bromopbenyl Phenyl Ether ND 10 033 3-Nitroanihne — 50 1 6 <br /> Butylbenzyl Phthalate ND 10 033 4-Nitroamlme -- 50 1 6 <br /> 4-Chloroanalme — 20 066 2-Nitrophenol ND 10 16 <br /> 4-Chioro-3-methy1pheno ND 5 033 4-Nttrophenol ND 10 1 6 <br /> 2-Chloronaphthalene ND 10 033 Nitrobenzene ND 10 033 <br /> 2-Chlorophenol ND 2 033 N-Nitrosodiphenylamine ND 1 033 <br /> 4-Chlorophenyl Phenyl Ether ND 5 033 N-Nitrosodi-n-propylarnme ND 5 033 <br /> Chrysene -- 10 033 Pentachlorophenol ND 1 16 <br /> Dibenzo(a,h)anthracene — 10 033 Phenanthrene -- 10 033 <br /> Dibenzofuran --- 10 0 33 Phenol ND 1 033 <br /> Di-n-butyl Phthalate ND 10 033 Pyrene --- 10 033 <br /> 1,2-Dichlorobenzene --- 10 033 1,2,4-Tnchlorobenzene --- 10 033 <br /> 1,3-Dichlorobenzene -- 10 033 2,4,5-Tnchlorophenol -- 10 033 <br /> 1,4-Dichlorobenzene -- 10 033 2,4,6-Tnchlorophenol ND 10 033 <br /> 3,3-Dichlorobenzidine ND 5 066 Di(2-ethylhexyl)adipate ND 5 <br /> 2,4-Dichlorophenol ND 1 0 33 Comments <br /> Diethyl Phthalate ND 2 033 Surrogate Recoveries(%) <br /> 2,4-Dimethylphenol ND 2 033 2-Fluorophenol 81 <br /> Dimethyl Phthalate ND 2 033 Phenol-d5 71 <br /> 4 6-Dinitro-2-methylphenol ND 10 16 Nitrobenzene-d5 88 <br /> 2,4-Dinitrophenol ND 5 16 2-Fluorobiphenyl 84 <br /> 2,4-Dmitrotoluene ND 5 033 2,4,6-Tnbromophenol 99 <br /> 2,6-Dmitrotoluene ND 5 033 p-Teiphenyt-d]4 56 <br /> *water samples are reported in ug/L,soil and sludge samples in mg/kg,wipes in ug/wipe and ail TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> • k surrogate diluted out of range <br /> h)lighter than water inumscible sheen is present,i)hquid sample that contains great than-5 vol %sediment, )sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />