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i <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> MCCI�MPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> httpa/www.i-nccaml)bcll.com E-mail:main@mccampbell.com <br /> IAdvanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 08/19/97 <br /> Date Received: 08/20/97 <br /> I 1803 West March Lane, Ste A <br /> Client Contact: Tim Cuellar Date Extracted: 08/20/97 <br /> Stockton, CA 95207 <br />' Client P.O: Date Analyzed: 08/20/97 <br /> Oxygenated Volatile Organics By GC/NIS <br /> EPA method 8260 modified <br /> I Lab ID 79925 79927 79929 79932 <br /> Reporting Limit <br /> Client ID P2-20 P2-30 P2-40 P1-23 to 27 <br />' Matrix S S S W S w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND ND 5.0 1.0 <br /> Ethanol ND ND ND ND 100 20 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methanol --- --- --- --- N/A NIA <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 410 50 5.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND 25 25 5.0 <br />' Surrogate Recoveries('%.) <br /> Dibromofluoromethane 96 95 101 103 <br />' Toluene-d8 101 102 103 98 <br /> Comments: —71 -1 <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ughvipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;0)sample diiuted due to <br /> high organic content <br /> 1 - <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />