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I 10 Second Avenue South,#137,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> 14 http://www.mccampbell.com E-mail: main@mccampbell.coni <br /> Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 08/19/97 <br /> Date Received: 08/20/97 <br /> 1803 West March Lane, Ste A <br /> Stockton,CA 95207 Client Contact: Tim Cuellar Date Extracted: 08/20/97 <br /> Client P.O: Date Analyzed: 08/20/97 <br /> Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab ID 79933 79934 79935 <br /> Reporting Limit <br /> Client ID P1-46 to 50 P2-20 to 24 P2-46 to 50 <br /> Matrix W w W $ W <br /> Compound Concentration* ug/kg uglL <br /> Di-isopropyl Ether(D1PE) ND ND ND 5.0 1.0 <br /> Ethanol ND ND ND 100 20 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND 5.0 1.0 <br /> Methanol --- --- --- NIA NIA <br /> Methyl-tert Butyl Ether(MTBE) 72 ND ND 50 5.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 5.0 1.0 <br /> tent-Butanol I ND ND 25 5.0 <br />' Surrogate Recoveries('%) <br /> Dibromofluoromethane 104 102 100 <br />' Toluene-d8 98 97 95 <br /> Comments: <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/S'rLC 1 SPLP extracts in uglL <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;0)sample diluted due to <br />' high organic content <br /> DHS Certification No. 1644 QC _Edward Hamilton, Lab Director <br /> 1 <br />