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I 1O Second Avenue South,#fD7, Pacheco,CA 94553 <br /> 4 MCCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax :510-798-1622 <br /> http://ivww.mccanipbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/05/97 <br /> 1803 West March Lane, Ste A Date Received: 09/09/97 <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/09/97 <br /> Client P.O: Date Analyzed: 09/10/97 <br /> Volatile Organics By GC/IVIS <br /> EPA method$260 <br /> Lab ID 80560 <br /> Client ID P4-20 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone" ND trans-1,3-Dichloropropene I ND <br /> Benzene ND Ethylene dibromide" ND <br /> Bromobenzene ND Ethylbenzene ND <br />' Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform • ND ]sopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br />' n-Butyl benzene ND Methyl butyl ketone 1° ND <br /> sec-Butyl benzene ND Methylcne Chloride"' ND <br /> Cert-Butyl benzene ND Methyl ethyl ketone"" ND <br /> Carbon Disulfide ND Methyl isobutvl ketone' ' ND <br /> Carbon Tetrachloride ND Methyl Cert-Butyl Ether(M'fBE) .-- <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene' ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1.2,2-,rctraclhloroetltaize ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br />' Dibromocmoromethane ND 1,2,3-"rrichlorobenze1le ND <br /> 1,2-Dibromo-3-chloropropane ND 1.2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1.1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> l,3-Dichlorobenzene, ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Triel110rOl1U01-0nlCthalle ND <br /> Dichlorodifluoromethane ND 1,23-Trichloropropane ND <br /> 1,1-Dichloroethane ND ],2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trinlethylbenzene ND <br /> 1,1-Dichioroethenc i ND Vinyl Acetate L" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride'°' ND <br /> trails-1,2-Dichloroethene ND Xylenes,total ND <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries('Y.,) <br /> 2,2-Diehl oropropane ND Dibromolluoromethane 99 <br /> 1,1-Dichloropropene ND Toluenc-d$ 102 <br /> cis-1,3-Dichloropropene ND 4-Bromoiluorobenzene 95 <br /> -water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wvipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanonc; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (I) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 i ,r Edward Hamilton, Lab Director <br />