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I 10 Second Avenue South,t#137,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> http://www.niecampbell.com E-mail: main a mccampbell.com <br /> Advanced GeoEnvironmentat Client Project ID: Flag City Chevron Date Sampled; 09/05/97 <br /> 1803 West March Lane, Ste A Date Received: 09/09/97 <br /> Stockton,CA 95207 <br /> Client Contact: Tim Cuellar Date Extracted: 09/09/97 <br /> Ghent P.O: Date Analyzed: 09/10/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 80562 <br /> Client ID P4-35 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> I AcetoneND trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> Bromobenzene ND Etbylbenzene ND <br /> Bromochlaromethane ND Hexachlorobutadiene ND <br />' Bromodicltloromethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"" ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND <br /> Cert-Butyl benzene ND Methyl ethyl ketone"' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone' ' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Fiher"I ND Styrene"' ND <br /> Chloroform ND 1,1,1,2-Tetrachloroelbane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroelhene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobcnzene ND <br /> Dibromomethane ND l,l,l-"Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,21'richloroethone ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br />' 1,4-Dichlorobenzene ND Trichlorolluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> ],I-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br />' 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"" ND <br /> trans-1,2-Dichloroethene ND Xylenes,total "' ND <br />' 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries('%) <br /> 2,2-Dichloropropane ND Dibromotluoromethane 106 <br /> l,l-Dichloropropene ND Toluene-d8 101 <br />' <br /> cis-1,3-Dichloropropene ND 4-2romoiluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples l ug/L;vapor samples 0.5 ug/L,solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br />' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) nrethyibertzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />