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METHOD SN50302608 • VOLATILE ORGANICS BY GC/MS Client HALEY 8 ALDRICH, INC. DateCollected 05/07/15 Project ABB STTOCKTON Date Received 05/08/15 Batch No 15EO45 Date Extracted 05/13/15 10:20 Sample ID SB-14-3.5-4.0 Date Analyzed 05/13/15 10:20 Lab Samp ID. E045-10R Dilution Factor. 0.92 Lab Fite ID: REP152 Matrix : SOIL Ext.Btch ID: VS02EO9 % Moisture : 19.1 CaLIb. Ref.: RDPO51 Instrument ID : T-002 S RL MDL PARAMETERS (ug%kg) (ug/kg) (ug/kg) ---------- _______ ....... _______ 1,1,1,2-TETRACHLOROETHANE NO 5.7 1.1 1,1,1-TRICHLOROE7HANE NO 5.7 1.1 1,1,2,2-TETRACHLOROETHANE ND 5.7 1.1 1,1,2-TRICHLOROETHANE NO 5.7 1.1 1,1-DICHLOROETHANE NO 5.7 1.1 1,1-DI CHLOROETHENE NO 5.7 1.1 1,1-DICHLOROPROPENE NO 5.7 1.1 1,2,3-TRICHLOROBENZENE NO 5.7 2. 1,2,3-TRICHLOROPROPANE NO 5.7 2. 1,2,4-TRICHLOROSENZENE ND 5.7 2.3 1,2,4-TR IMETHYLBENZENE ND 5.7 2.3 1,2-DIBROMO-3-CHLOROPROPANE ND 5.7 2.3 ,2-DIBROMOETHANE NO 5.7 1.1 1,2-DICHLOROBENZENE NO 5.7 1.1 1,2-DICHLOROETHANE NO 5.7 1.1 1,2-DICHLOROPROPANE NO 5.7 1.1 1,3,5-TRIMETHYLBENZENE NO 5.7 2.3 1,3-DICHLOROBENZENE NO 5.7 1.1 1,3-DICHLOROPROPANE NO 5.7 1.1 1,4-DICHLOROBENZENE NO 5.7 1.1 2,2-DICHLOROPROPANE NO 5.7 2.3 2-BUTANONE (MEK) 6.2J 11 5.7 2-CHLOROTOLUENE ND 5.7 1.1 2-HEXANONE NO 11 5.7 4--CHLOROTOLUENE NO 5.7 1.1 ACETONE 48 11 5.7 BENZENE 3.2J 5.7 1.1 BROMOBENZENE ND 5.7 1.1 BROMOCHLOROMETHANE ND 5.7 1.1 BROMODICHLOROMETHANE ND 5.7 1.1 BROMOFORM NO 5.7 2.3 BROMOMETHANE ND 11 2.3 CARBON DISULFIDE 6.3 5.7 1.1 CARBON TETRACHLORIDE NO 5.7 1.1 CHLOROBENZENE NO 5.7 1.1 CHLOROETHANE NO 5.7 2.3 CHLOROFORM ND 5.7 1.1 CHLOROMETHANE NO 5.7 2.3 CIS-1,2-DICHLOROETHENE NO 5.7 1.1 CIS-1 3-DICHLOROPROPENE NO 5.7 1.1 DBROAOCHLOROMETHANE NO 5.7 1.1 DIBROMOMETHANE NO 5.7 1.1 DICHLORODIFLUOROMETHANE NO 5.7 2.3 ETHYLBENZENE 4.OJ 5.7 1.1 HEXACHLOROBUTADIENE NO 5.7 2.3 ISOPROPYL BENZENE 2.BJ 5.7 2.3 M,P-XYLENES NO 11 2.3 4-METHYL-2-PENTANONE (MIBK) NO 11 5.7 METHYLENE CHLORIDE NO 11 2.3 METHYL-TERT-BUTYL ETHER (MTBE) NO 5.7 1.1 NAPHTHALENE 6.61 11 2.3 N-BUTYLBENZENE 1.31 5.7 1.1 N-PROPYLBENZENE NO 5.7 1.1 O-XYLENE NO 5.7 a.1 P-ISOPROPYLTOLUENE NO 5.7 I SEC-BUTYLBENZENE 3.3J 5.7 1.1 STYRENE ND 5.7 1.1 TERT-BUTYLBENZENE ND 5.7 1.1 TETRACHLOROETHENE ND 5.7 1.1 TOLUENE 1.91 5.7 1.1 TRANS-I,2-DICHLOROETHENE ND 5.7 1.1 TRANS-1 3-DICHLOROPROPENE NO 5.7 1.1 TRICHLOROETHENE NO 5.7 1.1 TRICHLOROFLUOROMETHANE ND 5.7 2.3 VINYL CHLORIDE ND 5.7 2.3 SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY QC LIMIT -------------------- ___-___ _.-=--- __________ ________ 1,2-DICHLOROETHANE-D4 57.9 56.86 102 60-160 4-BROMOFLUOROBENZENE 69.0 56.86 121" 85-120 TOLUENE-D8 6b.0 56.86 16" 85-115 DIBROMOFLUOROMETHANE 59.8 56.86 �05 70-130 20 7..3