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METHOD SI43559270C • <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> Client : HALEY 8 ALDRICH, INC. Date Collected: 05/07/15 <br /> Project : ABB STOCKTON Date Received: 05/08/15 <br /> Batch No. : 15EO45 Date Extracted: 05/11/15 11:45 <br /> Sample 10: SB-05-1.0-1.5 Date Analyzed: 05/11/15 18:08 <br /> Lab 5amp IDs E045.01 Dilution Factor. 1 <br /> Lab File ID: REJ133 Yamoisture : 17.9 <br /> Ext Btch ID: SVE006S Instrument ID i T-OE4 <br /> Calib. Ref.: RLJ013 <br /> RESULTS RL MDL <br /> PARAMETERS (ug/kg) (ug/kg) (ug/kg) <br /> ------- _-- <br /> 1,2,4-TRICHLOROBENZENE NO 410 200 <br /> 1,2-DICHLOROBENZENE NO 410 200 <br /> 1,2-DIPHENYLHYORAZINE (3) NO 470 200 <br /> 1,3-DICHLOROBENZENE , <br /> 200 <br /> 1,4-DICHLOROBENZENE <br /> 2,4,5-TRICHLOROPHENOLNO 410 200 200 <br /> 2,4,6-TRICHLOROPHENOL NO 4410 200 <br /> 10 200 <br /> 2,4-DICHLOROPHENOL <br /> 2,4-DIMETHYLPHENOL NO 810 200 <br /> 2,4-DINITROPHENOL <br /> 2,4-DI NITROTOLUENENO 410 200 NO 410 200 <br /> 2,6-DINITROTOLUENE 200 <br /> 2-CHLORONAPHTHALENE NO 410 <br /> 410 200 <br /> 2-CHLOROPHENOL <br /> 2-METHYLNAPHTHALENE NO 410 200 <br /> 2-METHYLPHENOL <br /> 2-NITROANILINE NO 410 200 <br /> 2-NITROPHENOL NO 410 200 <br /> 3,31-DICHLOROSENZIDINE NO 410 200 <br /> 4-MET HYLPHENOL (1) ND 470 200 <br /> 3-NITROANILINE. <br /> 4,6-DINITRO-2-METHYLPHENOL NO 810 200 <br /> 4-BROMOPHENYL-PHENYL ETHER NO 470 200 <br /> 4-CHLORO-3-METHYLPHENOL NO 410 200 <br /> 4 -CHLOROANILINE <br /> 4-CHLOROPHENYL-PHENYL ETHER NO 410 200 <br /> 410 200 <br /> 4-NITROANILINE <br /> 4-NITROPHENOL NO 810 200 <br /> ACENAPHTHENE NO 410 200 <br /> ACENAPHTHYLENE NO 4 0 200 <br /> ANTHRACENE NO 410 200 <br /> NO 410 200 <br /> BENZO(A)ANTHRACENE NO <br /> 00 <br /> BENZO(A)PYRENE <br /> BENZO(8)FLUORANTHENE NO 410 200 <br /> BENZO(G H I)PERYLENE N 410 200 <br /> BENZO(KSACID O 410 NTNENE NO 1600 8100 <br /> BENZOIC ACID NO 410 200 <br /> BENZYL ALCOHOL <br /> BIS(2-CHLOROISOPROPYL)ETHER NO 410 200 <br /> BIS(2-CHLOROETHOXY)METHANL NO 410 200 <br /> BIS(2-CHLOROETHYL)ETHER NO 410 200 <br /> BIS(2-ETHYLHEXYUPHT HALATENO 410 200 <br /> BUTYLBENZYLP HT HALATE NO 410 200 <br /> 410 200 <br /> CARBAZOLE <br /> 410 200 <br /> CHBYSENE <br /> DINO 410 200 <br /> DISENZOFENZO(A. H)ANTHRACENE AN NO 410 200 <br /> HTNA <br /> DIETHYLPHTNALATE NO 410 200 <br /> DIMETHYLPHTHALATE NO 410 200 <br /> 10 200 <br /> DI-N-BUTYLPHTHALATE <br /> FLUORACTYLPHTHALATE NO 410 10 200 <br /> FLUORANTNENE <br /> FLUORENE NO 410 200 <br /> HEXACHLOROBENZENE NO 410 200 <br /> HEXACHLOROBUTAOIENE NO 410 200 <br /> HEXACHLOR23-CDE NO 410 200 <br /> INDENO(1 2,3-CD)PYRENE NNO 410 O 410 200 <br /> IBOPHOROGE200 <br /> NAPHTHALENE NO 410 200 <br /> NITROBENZENE NO 410 410 200 <br /> N-NITROSODIMETHYLAMINE <br /> N-NITROSO-DI-N-PROPYLAMINE NO 410 200 <br /> N-NITROSODIPHENYLAMINE (2) <br /> PENTACHLOROPHENOL NO 810 200 <br /> PHENANTHRENE NO 410 200 <br /> PHENOL NO 410 NO 410 200 <br /> PYRENE <br /> SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY QC LIMIT <br /> _______ _______ __________ -------- <br /> 2,4 6-TRIBROMOPHENOL 1500 2436 61.6 35-125 <br /> 2 FLUOROBIPHENYL 541 812.1 66.6 45-105 <br /> 1330 2436 54.8 35-105 <br /> 2-FLUOROPHENOL <br /> NITROBENZENE-DS 513 812.1 63.2 35-100 <br /> PHENOL-D5 1548 81231 677.4 30-125 <br /> TERPNENYL-D 14 <br /> (1): Cannot be separated from 3:Methylphenol <br /> (2): Cannot be separated from Diphenytamine <br /> (3): 1,2 Diphenyloydrazine analyzed as Azobenzene due to decomposition in injector <br /> 3004 <br />