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METHOD SW3550B/8270C <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> Client HALEY & ALDRICH, INC. Date Collected 05/07/15 <br /> Project ABB STOCKTON Date Received 05/08/15 <br /> Batch No 15EO45 Date Extracted 05/11/15 11:45 <br /> Sample ID: SB-06-1.0-1.5 Date Analyzed. 05/11/15 18:27 <br /> Lab Samp ID: E045-02 Dilution Factor: 4.98 <br /> Lab File ID: REJ134 Matrix : SOIL <br /> Ext Btch ID: SVED06S % Moisture : 14.9 <br /> Calib. Ref:: RLJO13 Instrument ID : T-OE4 <br /> -------------------------------- <br /> RESULTS RL MDL <br /> PARAMETERS (ug/kg) (ug/kg) (ug/kg) <br /> ---------- ------- ------- _______ <br /> 1,2,4-TRICHLOROSENZENE ND 1900 980 <br /> 1,2-DICHLOROBENZENE ND 1900 980 <br /> 1,2-DIPHENYLHYDRAZINE (3) NO 1900 980 <br /> 1,3-DICHLOROBENZENE NO 1900 980 <br /> 1,4-DICHLOROBENZENE NO 1900 980 <br /> 2,4,5-TRICHLOROPHENOL NO 1900 980 <br /> 2,4,6-TRICHLOROPHENOL NO 1900 980 <br /> 2,4-DICHLOROPHENOL NO 1900 980 <br /> 2,4-DIMETHYLPHENOL ND 1900 980 <br /> 2,4-DINITROPHENOL ND 3900 980 <br /> 2,4-DINITROTOLUENE NO 1900 980 <br /> 2,6-DINITROTOLUENE NO 1900 980 <br /> 2-CHLORONAPHTHALENE NO 1900 980 <br /> 2-CHLOROPHENOL NO 1900 980 <br /> 2-METHYLNAPHTHALENE NO 1900 980 <br /> 2-METHYLPHENOL NO 1900 980 <br /> 2-NITROANILINE ND 1900 980 <br /> 2-NITROPHENOL ND 1900 980 <br /> 3,31-DICHLOROBENZIDINE ND 1900 980 <br /> 4-METHYLPHENOL (1) ND 1900 980 <br /> 3-NITROANILINE ND 1900 980 <br /> 4,6-DINITRO-2-METHYLPHENOL ND 3900 980 . <br /> 4-BROMOPHENYL-PHENYL ETHER NO 1900 980 <br /> 4-CHLORO-3-METHYLPHENOL NO 1900 980 <br /> 4-CHLOROANILINE NO 1900 980 <br /> 4-CHLOROPHENYL-PHENYL ETHER NO 19DO 980 <br /> 4-NITROANILINE NO 1900 980 <br /> 4-NITROPHENOL ND 3900 980 <br /> ACENAPHTHENE ND 1900 980 <br /> ACENAPHTHYLENE NO 1900 980 <br /> ANTHRACENE ND 1900 980 <br /> BENZO(A)ANTHRACENE 1200J 1900 980 <br /> BENZO(A)PYRENE 19001 1900 980 <br /> BENZO(B)FLUORANTHENE - 2000 1900 980 <br /> BENZO(G H I)PERYLENE 1400J 1900 980 <br /> BENZO(K$FMRANTHENE NO 1900 980 <br /> BENZOIC ACID NO 7800 3900 <br /> BENZYL ALCOHOL ND 1900 980 <br /> BIS(2-CHLOROISOPROPYL)ETHER ND 1900 980 <br /> BIS(2-CHLOROETHOXY)METHANE NO 1900 980 <br /> BIS(2-CHLOROETHYL)ETHER ND 1900 980 <br /> BIS(2-ETHYLHEXYL)PHTHALATE NO 1900 980 <br /> BUTYLBENZYLPHTHALATE NO 1900 980 <br /> CARBAZOLE NO 1900 980 <br /> CHRYSENE 15001 1900 980 <br /> DIBENZO(A H)ANTHRACENE NO 1900 980 <br /> DIBENZOFUkAN. NO 1900 980 <br /> DIETHYLPHTHALATE NO 1900 980 <br /> DIMETHYLPHTHALATE ND 1900 980 <br /> DI-N-BUTYLPHTHALATE NO 1900 980 <br /> DI-N-OCTYLPHTHALATE ND 1900 980 <br /> FLUORANTHENE 3100 1900 980 <br /> FLUORENE ND 1900 980 <br /> HEXACHLOROBFNZENE ND 1900 980 <br /> HEXACHLOROBUTADIENE ND 1900 980 <br /> HEXACHLOROETHANE NO 1900 980 <br /> INDENO(1 2,3-CD)PYRENE 1000J 1900 980 <br /> ISOPHOROIIE NO 1900 980 <br /> NAPHTHALENE ND 1900 980 <br /> NITROBENZENE NO 1900 980 <br /> N-NITROSODIMETHYLAMINE NO 1900 980 <br /> N-NITROSO-DI-N-PROPYLAMINE NO 1900 980 <br /> N-NITROSODIPHENYLAMINE (2) NO 1900 980 <br /> PENTACHLOROPHENOL ND 3900 980 <br /> PHENANTHRENE 2200 1900 980 <br /> PHENOL ND 1900 980 <br /> PYRENE 4100 1900 980 <br /> SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY OC LIMIT <br /> ---------- --------- ------- ___v___ .......... -------- <br /> 2,4 6-TRIBROMOPHENOL 7390 11690 63.2 35-125 <br /> 2`-FLUOROBIPHENYL 2670 3898 68.5 45-105 <br /> 2-FLUOROPHENOL 6320 11690 54.0 35-105 <br /> NITROBENZENE-D5 2380 3898 61.1 35-100 <br /> PHENOL-05 7070 11690 60.4 40-100 <br /> TERPHENYL-D14 2830 3898 72.6 30-125 <br /> (1): Cannot be separated from 3-MethylphenoL <br /> (2): Cannot be separated from Diphenylamine <br /> (3): 1,2 Diphenylhydrazine analyzed as Azobenzene due to decomposition in injector <br /> -admf:3g-- <br />