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METHOD SLf3550B/8270C • <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> Client HALEY & ALDRICH, INC. Date Collected 05/06/15 <br /> Project ABB STOCKTON Date Received 05/07/15 <br /> Batch No 15E022 Date Extracted 05/11/15 11:45 <br /> Sample ID. SB^01-1.0-1.5DL Date Analyzed. 05/12/15 13:20 <br /> Lab Sainp. ID: E022-011 Dilution Factor: 49.8 <br /> Lab File ID: REJ148 Matrix : SOIL <br /> Ext Btch ID: SVE006S % Moisture : 13.1 <br /> CaLib. Ref.: RLJO13 Instrument ID : T-OE4 <br /> PARAMETERS (ug/kg) (ug/kg) (ug/kg) <br /> __________ _______ _______ ....... <br /> 1,2,4-TRICHLOROBENZENE NO 19000 9600 <br /> 1,2-DICHLOROBENZENE ND 19000 9600 <br /> 1,2-DIPHENYLHYDRAZINE (3) NO 19000 9600 <br /> 1,3-DICHLOROBENZENE NO 19000 9600 <br /> 1,4-DICHLOROBENZENE NO 19000 9600 <br /> 2,4,5-TRICHLOROPHENOL NO 19000 9600 <br /> 2,4,6-TRICHLOROPHENOL NO 19000 9600 <br /> 2,4-DICHLOROPHENOL NO 19000 9600 <br /> 2,4-DIMETHYLPHENOL ND 19000 9600 <br /> 2,4-DINITROPHENOL NO 38000 9600 <br /> 2,4-DINITROTOLUENE NO 19000 9600 <br /> 2_,6-DINITROTOLUENE NO 19000 9600 <br /> 2-CHLORONAPHTHALENE NO 19000 9600 <br /> 2-CHLOROPHENOL NO 19000 9600 <br /> 2-METHYLNAPHTHALENE ND 19000 9600 <br /> 2-METHYLPHENOL ND 19000 9600 <br /> 2-NITROANILINE NO 19000 9600 <br /> 2-NITROPHENOL NO 19000 9600 <br /> 3,3.--DICHLOROBENZIDINE ND 19000 9600 <br /> 4-ME <br /> THYLPHENOL (1) NO 19000 9600 <br /> 3-NITROANILINE NO 19000 9600 <br /> 4,6-DINITRO-2-METHYLPHENOL NO 38000 9600 <br /> 4-BROMOPHENYL-PHENYL ETHER NO 19000 9600 <br /> 4-CHLORO-3-METHYLPHENOL NO 19000 9600 <br /> 4-CHLOROANILINE NO 19000 9600 <br /> 4-CHLOROPHENYL-PHENYL ETHER NO 19000 9600 <br /> 4-NITROANILINE NO 19000 9600 <br /> 4-NITROPHENOL NO 38000 9600 <br /> ACENAPHTHENE NO 19000 9600 <br /> ACENAPHTHYLENE NO 19000 9600 <br /> ANTHRACENE NO 19000 9600 <br /> BENZO(A)ANTHRACENE 28000 19000 9600 <br /> BENZO(A)PYRENE 55000 19000 9600 <br /> BENZO(B)FLUORANTHENE 63000 19000 9600 <br /> BENZO(G H I)PERYLENE 69000 19000 9600 <br /> BENZO(KSFLUORANTHENE 13000J 19000 9600 <br /> BENZOIC ACID NO 76000 38000 <br /> BENZYL ALCOHOL NO 19000 9600 <br /> BIS(2-CHLOROISOPROPYL)ETHER NO 19000 9600 <br /> BIS(2-CHLOROETHOXY)METHANE NO 19000 9600 <br /> BIS(2-CHLOROETHYL)ETHER NO 19000 9600 <br /> BIS(2-ETHYLHEXYL)PHTHALATE ND 19000 9600 <br /> BUTYLBENZYLPHTHALATE NO 19000 9600 <br /> CARBAZOLE NO 19000 9600 <br /> CHRYSENE 40000 19000 9600 <br /> DIBENZO(A H)ANTHRACENE NO 19000 9600 <br /> DISENZOFUAAN NO 19000 9600 <br /> DIETHYLPHTHALATE NO 19000 9600 <br /> DIMETHYLPHTHALATE NO 19000 9600 <br /> DI-N-BUTYLPHTHALATE NO 19000 9600 <br /> DI-N-OCTYLPHTHALATE NO 19000 9600 <br /> FLUORANTHENE 90000 19000 9600 <br /> FLUORENE NO 19000 9600 <br /> HEXACHLOROBENZENE NO 19000 9600 <br /> HEXACHLOROBUTADIENE ND 19000 9600 <br /> HEXACHLOROETHANE NO 19000 9600 <br /> INDENO(1 2,3-CD)PYRENE 47000 19000 9600 <br /> ISOPHOROAE ND 19000 9600 <br /> NAPHTHALENE NO 19000 9600 <br /> NITROBENZENE NO 19000 9600 <br /> N-NITROSODIMETHYLAMINE NO 19000 9600 <br /> N-NITROSO-DI-N-PROPYLAMINE NO 19000 9600 <br /> N-NITROSODIPHENYLAMINE (2) NO 19000 9600 <br /> PENTACHLOROPHENOL NO 38000 9600 <br /> PHENANTHRENE 53000 19000 9600 <br /> PHENOL ND 19000 9600 <br /> PYRENE 110000 19000 9600 <br /> SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY OC LIMIT <br /> ____________________ ...... ---_--- ---------- ----_... <br /> 2,4 6-TRIBROMOPHENOL 7220 11450 63.1 35-125 <br /> 2-FLUOROBIPHENYL 2890 3817 75.7 45-105 <br /> 2-FLUOROPHENOL 6650 11450 58.1 35-105 <br /> NITROBENZENE-D5 2540 3817 66.5 35-100 <br /> PHENOL-D5 7320 11450 63.9 40-100 <br /> TERPHENYL-D14 3120 3817 81.7 30-125 <br /> (1): Cannot be separated from 3-MethylphenoL <br /> (2): Cannot be separated from DiphenyLamine <br /> (3): 1,2 DiphenylMrazine analyzed as Azobenzene due to decomposition in injector <br />