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METHOD S1135 68270C • <br /> SEMI VOLATILE ORGANICS BY GC/MS <br /> __________________________________________________________ <br /> Client : HALEY7& ALDRICH, INC. Date Cc' <br /> legtad• pgIll <br /> Project : A B OCKTON Date Rceive Batch No 1 Epp8 Date Extr cte g gi1s`455 <br /> Lab' Samp ID. E022-04•5 gE022-041 MMDalutionnFactor: . 9.8:50 # 05/12/15 13:40 <br /> Lab File to: REJ77zz REJ149 %aMoisture c 22 2 <br /> Ext_Btch ID: SVESO¢S <br /> Caleb. Ref.: RLJ 771133 Instrument ID T-OE4 <br /> PARAMETERS (ug%kg (ug/kg (ug/kg) <br /> 1, ,4-TRICHLOROBENZENE No § OQ IDD <br /> 77 DICHLOROBENZENE ND 4Zr9 Ou o <br /> ll-'DICHLOROBENZENE <br /> (3) No 00 IN <br /> 1111 -DICHLOROBENZENE ND 00 ,I <br /> 1',�:�!TRHLOROBENZENE ND 00;6-TICHLOROPIC HENOL ND qq 00 100 <br /> ,4-DICHLOROPHENOL ND 4 00 1100 <br /> 44-DIMETHYLPHENOL ND 4 0 100 <br /> ,4-DINITROPHENOL ND 8 00 100 <br /> 4-DINITROTOLUENE ND 00 100 <br /> 6-DINITROTOLUENE ND 00 100 <br /> =CHLORONAPHTHALENE ND DO 100 <br /> -CHLOROPHENOL ND 00 100 <br /> -METHYLNAPHTHALENE ND 0 100 <br /> -METHYLPHENOL ND 0 2100 <br /> -NITROANILINE ND 0 100 <br /> NITROPHENOL ND 0 <br /> 3'-DICHLOROBENZIDINE ND 00 7 100 <br /> -MMNETHYLPHENOL (1) ND 00 100 <br /> 5,6!DINITROI2EMETHYLPHENOL ND 8 00 100 <br /> 4-BROMOPH NYL-PHENYL ETHER ND 0 100 <br /> 4-C LORO-33EE-METHYLPHENOL NO QQQQ i] <br /> 4-CHLOROANILINE NO 80 D <br /> l4. CHLOROPHENY PHENYL ETHER ND 88 8 <br /> 4-NITROPHENOLE ND 8q 00 10 <br /> ACENAPHTHENE NO 00 100 <br /> ACENAPHTHYLENE ND 4 a 00 �00 <br /> ANTHRACENE 3 No 0 <br /> BENZOt((A33ANTHRACENE 3334000 D0 1800 <br /> # <br /> BENZO <br /> 8)FLUORANTHENE 35000 2 00 1 0p00 <br /> BEN20 G H I PERYLENE 1$000 4 00 [00 <br /> BE KWUORANTHENE !!,, <br /> BE C ACID ND 17 0Q 5 0 <br /> BENZYL ALCOHOL T ND Yj OU ��0 <br /> SIS(1_CHLOROISOPROPYL ETHER ND 0 <br /> BIS(((ztz CHLOROETHOXY)ME HANE ND 00 71 0 <br /> BI B[2-ETNOYLHEXYLt HTHALATE ND 00 100 <br /> BUT LBENZYLPHTHA ATE ND 00 00 <br /> CARBAZOLE N 00 00 <br /> # CHRYSENE 44000 2 00 1 00 <br /> DIBENZO((A H)ANTHRACENE ND DO 100 <br /> DIBENZOFUAAN ND 00 10 <br /> DIETHYLPHTHALATE ND 00 100 <br /> DIMETHYLPHTHALATE NO 0 1100 <br /> DI-N-BUTYLPHT NALATE ND 00 10 <br /> FLUORANTHENETHAI.ATE 20000 00 2100 <br /> FLUORENE No00� 00 <br /> HEXACHLOROBENZENE ND <br /> HEXACHLOROBUTADIENE ND 00 7100 <br /> HEXACHLOROETHANE ND 100 <br /> INDENO 11 22 33 CD)PYRENE 12000 'u� <br /> ISOPHO OWE' ND 100 <br /> NAPHTHALENE NO 00 { <br /> NITROBENZENE ND 00 8 <br /> N -NITROSODIMETHYLAMINE ND <br /> N-NITROSO-DI-N-PROPYLAMINE ND <br /> N-NITROSODIPHENYLAMINE (2) ND 00 0 <br /> PENTACHLOROPHENOL ND 00 1 0 <br /> PHENANTHRENE 7000 00 �00 <br /> # PYRENE 41000 2 00 1 000 <br /> SURROGATE PARAMETERS RESULTS SPK-.AMT X RECOVERY OC LIMIT <br /> -------------------- _--____ ___ _.__ __________ ______,- <br /> 22 4 6-TRIBROMOPHENOL q 0 1 0 �$•7 J5':J25 <br /> 2FCUOR00]PHENYL 30 470 <br /> 2222-FLUOROPHENOL gg 0 7z 5- 5 <br /> NITROBENZENE-D5 g0 0 4 70 72.1 5-9 <br /> p zZTERPHENYL-D14 72760 174 70 67467333 50-171725 <br /> # 2-FLUOROPHENOOPHENOL 2920 ;2 B 50.3 5- 05 <br /> FLUOROB)PNENYL g7g7$ �a g <br /> # NITROBENZENE-DS 0040 12810 ;1 30. 25 <br /> # <br /> PHENOL-DD <br /> # TERPHENYL-014 3120 4270 <br /> # Members of the Associated File <br /> 1): Cannot be separated from 3-MethyLphenoL <br /> 2 : Cannot yheseparateSl from i henylamine <br /> 3�: 1,2 Dip henylhydrazine anaQyied as Azobenzene due to decomposition in injector <br />