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COLUMBIA ANALYTICAL SERVICES,INC. <br /> QA/QC Report <br /> Client Equiva Services Service Request: S9901977 <br /> Prosect: SAP 121258/Incident 88870583 Date Collected: NA <br /> Sample Matrix: Soil Date Received: NA <br /> Date Extracted: NA <br /> Date Analyzed NA <br /> Surrogate Recovery Summary <br /> TPH as Gasoline <br /> Prep Method EPA 5030 Units PERCENT <br /> Analysis Method CA/LUFT Basis NA <br /> Test Percent Recovery <br /> Sample Name Lab Code Notes a,a,a-Tnfluorotoluene <br /> SP-IA S9901977-001 101 <br /> SP-1B 59901977-002 84 <br /> SP-2A S9901977-003 90 <br /> SP-2B S9901977-004 98 <br /> SP-3A S9901977-005 94 <br /> SP-3B 59901977-006 96 <br /> SP-4A S9901977-007 95 <br /> SP-4B 59901977-008 97 <br /> SP-SA 59901977-009 99 <br /> SP-5B 59901977-010 97 <br /> SP-6A S9901977-011 92 • <br /> SP-6B S9901977-012 94 <br /> SP-7A S9901977-013 99 <br /> SP-7B S9901977-014 102 <br /> SP-8A S9901977-015 100 <br /> SP-813 S9901977-016 99 <br /> SP-9A S9901977-017 93 <br /> SP-913 S9901977-018 96 <br /> _ Method Blank -- - -- 5990630-SBI _ _ _ _- _ _ _ t y _ 108- <br /> Method Blank 5990630-SB2 108 <br /> SP-IA 59901977-001 MS III <br /> SP-IA S9901977-001 DMS 108 <br /> CAS Acceptance Limits 51-137 <br /> Approved By Date <br /> SUR 1/020597p <br /> Page 1 I <br />