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COLUMBIA ANALYTICAL SERVICES, INC. <br /> QA/QC Report <br /> Client- Equrva Services Service Request. 59901977 <br /> Project SAP 121258/Incident 88870583 Date Collected. NA <br /> Sample Matrix. Solt Date Received: NA <br /> Date Extracted. NA <br /> Date Analyzed NA <br /> Surrogate Recovery Summary <br /> TPH as Gasolme <br /> Prep Method EPA 5030 Units PERCENT <br /> Analysis Method CA/LUFT Basis NA <br /> Test Percent Recovery <br /> Sample Name Lab Code Notes a,a,a-Trlfluorotoluene <br /> SP-IOA S9901977-019 102 <br /> SP-1013 59901977-020 98 <br /> SP-11A 59901977-021 <br /> 97 <br /> SP-1113 S9901977-022 89 <br /> SP-12A 59901977-023 97 <br /> SP-1213 59901977-024 <br /> 99 <br /> SP-13A 59901977-025 92 <br /> SP-13B 59901977-026 106 <br /> SP-14A 59901977-027 87 <br />. SP-14B 59901977-028 91 <br /> SP-15A S9901977-029 98 <br /> SP-15B 59901977-030 97 <br /> SP-16A 59901977-031 <br /> 10] <br /> SP-16B 59901977-032 99 <br /> SP-17A 59901977-033 103 <br /> SP-17B 59901977-034 96 <br /> SP-ISA 59901977-035 <br /> 102 <br /> SP-1813 59901977-036 90 <br /> SP-9A 59901977-0017MS 101 <br /> SP-9A 59901977-0017DMS 106 <br /> CAS Acceptance Linuts 51-137 <br /> Approved By T Date <br /> SUR 11020597p <br />